Information card for entry 7115124

Structure parameters

• Formula: C44 H40 Cl4 N4 O P2 Re
• Calculated formula: C44 H40 Cl4 N4 O P2 Re
• Title of publication: Oxygen atom transfer from RevO to tertiary diphosphines: spacer length and chemical differentiation of products
• Authors of publication: Bhattacharyya, Sibaprasad; Chakraborty, Indranil; Dirghangi, Bimal Kumar; Chakravorty, Animesh
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 18
• Pages of publication: 1813
• a: 10.11 ± 0.006 Å
• b: 10.668 ± 0.005 Å
• c: 20.76 ± 0.007 Å
• α: 89.47 ± 0.03°
• β: 80.08 ± 0.04°
• γ: 81.41 ± 0.04°
• Cell volume: 2180.5 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0755
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for all reflections: 0.1477
• Weighted residual factors for significantly intense reflections: 0.1279
• Goodness-of-fit parameter for all reflections: 1.07
• Goodness-of-fit parameter for significantly intense reflections: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No