Information card for entry 7116210

Structure parameters

• Common name: tetramethylammonium bisantimonydodecaniobophosphate
• Formula: C104 H264 N26 Nb36 O209 P3 Sb6
• Calculated formula: C104 H264 N26 Nb36 O209.102 P3 Sb6
• Title of publication: Reversible capping/uncapping of phosphorous-centered Keggin-type polyoxoniobate clusters.
• Authors of publication: Son, Jung-Ho; Casey, William H.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 8
• Pages of publication: 1436 - 1438
• a: 13.5271 ± 0.0006 Å
• b: 15.379 ± 0.0007 Å
• c: 38.1915 ± 0.0018 Å
• α: 95.015 ± 0.001°
• β: 93.776 ± 0.001°
• γ: 93.571 ± 0.001°
• Cell volume: 7879 ± 0.6 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0495
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.102
• Weighted residual factors for all reflections included in the refinement: 0.1036
• Goodness-of-fit parameter for all reflections included in the refinement: 1.162
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No