Information card for entry 7116284

Structure parameters

• Formula: C68 H64 B Cl2 Cu3 F4 N2 P6
• Calculated formula: C68 H64 B Cl2 Cu3 F4 N2 P6
• Title of publication: Organometallic polyphosphorus and -arsenic ligands as linkers between pre-assembled linear Cu(I) fragments.
• Authors of publication: Fleischmann, Martin; Dütsch, Luis; Moussa, Mehdi Elsayed; Schindler, Andrea; Balázs, Gábor; Lescop, Christophe; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 14
• Pages of publication: 2893
• a: 12.7414 ± 0.0004 Å
• b: 13.4211 ± 0.0004 Å
• c: 21.404 ± 0.0007 Å
• α: 85.562 ± 0.003°
• β: 72.949 ± 0.003°
• γ: 79.079 ± 0.003°
• Cell volume: 3435 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0831
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for significantly intense reflections: 0.1417
• Weighted residual factors for all reflections included in the refinement: 0.1549
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No