Information card for entry 7116626

Structure parameters

• Formula: C30 H46 Ge2 N4 Se3
• Calculated formula: C30 H46 Ge2 N4 Se2.607
• Title of publication: Single-step conversion of silathiogermylene to germaacid anhydrides: unusual reactivity
• Authors of publication: Surendar Karwasara; Dhirendra Yadav; Chandan Kumar Jha; Gopalan Rajaraman; Selvarajan Nagendran
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 4310
• a: 16.736 ± 0.003 Å
• b: 11.336 ± 0.002 Å
• c: 18.978 ± 0.003 Å
• α: 90°
• β: 106.354 ± 0.003°
• γ: 90°
• Cell volume: 3454.8 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0545
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1169
• Weighted residual factors for all reflections included in the refinement: 0.1329
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No