Information card for entry 7116998

Structure parameters

• Formula: C36 H36 As Cl2 N Si
• Calculated formula: C36 H36 As Cl2 N Si
• Title of publication: Utilisation of a lithium boryl as a reducing agent in low oxidation state group 15 chemistry: synthesis and characterisation of an amido-distibene and a boryl-dibismuthene
• Authors of publication: Deepak Dange; Amelia Davey; Joseph A. B. Abdalla; Simon Aldridge; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 7128
• a: 8.8947 ± 0.0005 Å
• b: 12.7255 ± 0.0008 Å
• c: 15.2825 ± 0.0009 Å
• α: 78.686 ± 0.003°
• β: 73.993 ± 0.003°
• γ: 70.48 ± 0.003°
• Cell volume: 1556.81 ± 0.16 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0825
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No