Information card for entry 7117005

Structure parameters

• Formula: C63.5 H73.5 As B N3 Si
• Calculated formula: C63.5 H73.5 As B N3 Si
• Title of publication: Utilisation of a lithium boryl as a reducing agent in low oxidation state group 15 chemistry: synthesis and characterisation of an amido-distibene and a boryl-dibismuthene
• Authors of publication: Deepak Dange; Amelia Davey; Joseph A. B. Abdalla; Simon Aldridge; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 7128
• a: 12.3574 ± 0.001 Å
• b: 12.667 ± 0.001 Å
• c: 19.7946 ± 0.0018 Å
• α: 99.963 ± 0.007°
• β: 104.228 ± 0.007°
• γ: 100.574 ± 0.007°
• Cell volume: 2874 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1896
• Residual factor for significantly intense reflections: 0.1023
• Weighted residual factors for significantly intense reflections: 0.254
• Weighted residual factors for all reflections included in the refinement: 0.3149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No