Information card for entry 7117008

Structure parameters

• Formula: C52 H72 B2 Bi2 N4
• Calculated formula: C52 H72 B2 Bi2 N4
• Title of publication: Utilisation of a lithium boryl as a reducing agent in low oxidation state group 15 chemistry: synthesis and characterisation of an amido-distibene and a boryl-dibismuthene
• Authors of publication: Deepak Dange; Amelia Davey; Joseph A. B. Abdalla; Simon Aldridge; Cameron Jones
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 7128
• a: 10.501 ± 0.0007 Å
• b: 12.7973 ± 0.0014 Å
• c: 21.8679 ± 0.0009 Å
• α: 88.502 ± 0.005°
• β: 76.645 ± 0.004°
• γ: 67.584 ± 0.008°
• Cell volume: 2636.9 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0902
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No