Information card for entry 7117313

Structure parameters

• Chemical name: 6-acetylimidazo[1,2-a]pyridine-2,3-diyl)bis(phenylmethanone)
• Formula: C23 H16 N2 O3
• Calculated formula: C23 H16 N2 O3
• SMILES: O=C(c1ccccc1)c1nc2n(cc(C(=O)C)cc2)c1C(=O)c1ccccc1
• Title of publication: Cu(OAc)2-Et3N mediated oxidative coupling of alpha-azido ketones with pyridinium ylides: utilizing in situ generated imines for regioselective synthesis of imidazo[1,2-a]pyridines
• Authors of publication: Ahmed Kamal; Chada Narsimha Reddy; Malasala Satyaveni; D. Chandrasekhar; Jagadeesh Babu Nanubolu; Kiran Kumar Singarapud; Ram Awatar Maurya
• Journal of publication: Chem.Commun.
• Year of publication: 2015
• Journal volume: 51
• Pages of publication: 10475
• a: 26.382 ± 0.003 Å
• b: 8.7432 ± 0.0009 Å
• c: 15.937 ± 0.0016 Å
• α: 90°
• β: 97.035 ± 0.002°
• γ: 90°
• Cell volume: 3648.4 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0341
• Weighted residual factors for significantly intense reflections: 0.094
• Weighted residual factors for all reflections included in the refinement: 0.1009
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No