Information card for entry 7118043

Structure parameters

• Formula: C18 H42 N6 P4
• Calculated formula: C18 H42 N6 P4
• Title of publication: Steric C-N bond activation on the dimeric macrocycle [{P(μ-NR)}2(μ-NR)]2.
• Authors of publication: Shi, Yan X.; Liang, Rong Z.; Martin, Katherine A.; Star, Daniel G.; Díaz, Jesús; Li, Xin Y.; Ganguly, Rakesh; García, Felipe
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2015
• Journal volume: 51
• Journal issue: 92
• Pages of publication: 16468 - 16471
• a: 8.9073 ± 0.0011 Å
• b: 15.7025 ± 0.0018 Å
• c: 9.9032 ± 0.0011 Å
• α: 90°
• β: 113.061 ± 0.004°
• γ: 90°
• Cell volume: 1274.4 ± 0.3 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1459
• Residual factor for significantly intense reflections: 0.0691
• Weighted residual factors for significantly intense reflections: 0.1467
• Weighted residual factors for all reflections included in the refinement: 0.1835
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No