Information card for entry 7118392

Structure parameters

• Formula: Cs1.5 H130 Na14.5 Ni7 O180 P4 W30
• Calculated formula: Cs0.5 Na11.6 Ni7 O160 P4 W30
• Title of publication: Heptanickel(ii) double-cubane core in wells-dawson heteropolytungstate, [Ni7(OH)6(H2O)6(P2W15O56)2](16.).
• Authors of publication: Bassil, Bassem S.; Xiang, Yixian; Haider, Ali; Hurtado, Jaime; Novitchi, Ghenadie; Powell, Annie K.; Bossoh, A. Martin; Mbomekallé, Israël M; de Oliveira, Pedro; Kortz, Ulrich
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 12
• Pages of publication: 2601 - 2604
• a: 12.7488 ± 0.0004 Å
• b: 12.7765 ± 0.0004 Å
• c: 25.7791 ± 0.001 Å
• α: 92.399 ± 0.002°
• β: 101.831 ± 0.002°
• γ: 104.172 ± 0.002°
• Cell volume: 3966 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.154
• Weighted residual factors for all reflections included in the refinement: 0.1678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No