Crystallography Open Database

Information card for entry 7119278

7119277 << 7119278 >> 7119279

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Coordinates	7119278.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C247 H240 Cl4 La4 N16 O8
Calculated formula	C247 H240 Cl4 La4 N16 O8
Title of publication	Bis(amidinate) ligands in early lanthanide chemistry - synthesis, structures, and hydroamination catalysis.
Authors of publication	Kazeminejad, Neda; Munzel, Denise; Gamer, Michael T.; Roesky, Peter W.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2017
Journal volume	53
Journal issue	6
Pages of publication	1060 - 1063
a	21.2533 ± 0.0004 Å
b	21.617 ± 0.0004 Å
c	25.3669 ± 0.0005 Å
α	75.244 ± 0.001°
β	83.199 ± 0.002°
γ	82.524 ± 0.002°
Cell volume	11129.9 ± 0.4 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1508
Residual factor for significantly intense reflections	0.0879
Weighted residual factors for significantly intense reflections	0.2243
Weighted residual factors for all reflections included in the refinement	0.2794
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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