Crystallography Open Database

Information card for entry 7119518

7119517 << 7119518 >> 7119519

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Coordinates	7119518.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H102 Mo3 N8 O14 V4
Calculated formula	C67.9 H102 Mo3 N8 O14 V4
Title of publication	[V4Mo3O14(NAr)3(μ2-NAr)3](2-): the first polyarylimido-stabilized molybdovanadate cluster.
Authors of publication	Huang, Yichao; Zhang, Jiangwei; Ge, Jingxuan; Sui, Chong; Hao, Jian; Wei, Yongge
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2017
Journal volume	53
Journal issue	17
Pages of publication	2551 - 2554
a	13.4643 ± 0.0007 Å
b	16.5903 ± 0.0011 Å
c	21.0115 ± 0.0014 Å
α	107.438 ± 0.006°
β	92.843 ± 0.005°
γ	108.583 ± 0.005°
Cell volume	4189.3 ± 0.5 Å³
Cell temperature	98 ± 5 K
Ambient diffraction temperature	98 ± 5 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0584
Residual factor for significantly intense reflections	0.0424
Weighted residual factors for significantly intense reflections	0.0975
Weighted residual factors for all reflections included in the refinement	0.1011
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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