Information card for entry 7119539

Structure parameters

• Formula: C100 H150 O16 Os8 S16
• Calculated formula: C93.5 O8 Os4 S8
• Title of publication: Wheel-to-rhomboid isomerization as well as nitrene transfer catalysis of ruthenium-thiolate wheels.
• Authors of publication: Tso, Ken Chi-Hang; Chan, Sharon Lai-Fung; Huang, Jie-Sheng; Che, Chi-Ming
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 16
• Pages of publication: 2419 - 2422
• a: 15.4686 ± 0.0019 Å
• b: 17.485 ± 0.002 Å
• c: 19.258 ± 0.002 Å
• α: 72.157 ± 0.004°
• β: 88.111 ± 0.005°
• γ: 73.892 ± 0.005°
• Cell volume: 4755.8 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0547
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1318
• Weighted residual factors for all reflections included in the refinement: 0.1397
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No