Information card for entry 7119714

Structure parameters

• Formula: C39 H49 N3 Pb
• Calculated formula: C39 H49 N3 Pb
• SMILES: [Pb]1N(c2c(N1c1c(cccc1C(C)C)C(C)C)cccc2)c1c(cccc1C(C)C)C(Nc1c(cc(cc1C)C)C)(C)C
• Title of publication: Reactivity of heavy carbene analogues towards oxidants: a redox active ligand-enabled isolation of a paramagnetic stannylene.
• Authors of publication: Janes, Trevor; Zatsepin, Pavel; Song, Datong
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2017
• Journal volume: 53
• Journal issue: 21
• Pages of publication: 3090 - 3093
• a: 11.2497 ± 0.0008 Å
• b: 22.1876 ± 0.0018 Å
• c: 13.7655 ± 0.001 Å
• α: 90°
• β: 93.6 ± 0.003°
• γ: 90°
• Cell volume: 3429.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.0263
• Weighted residual factors for significantly intense reflections: 0.0498
• Weighted residual factors for all reflections included in the refinement: 0.0535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No