Information card for entry 7120537

Structure parameters

• Formula: C28 H46 Co2 F12 N2 P2 S2
• Calculated formula: C28 H46 Co2 F12 N2 P2 S2
• Title of publication: Migratory Insertion and Hydrogenation of a Bridging Azide in Thiolate-Bridged Dicobalt Reaction Platform
• Authors of publication: Zhang, Yixin; Tong, Peng; Yang, Dawei; Li, Jianzhe; Wang, Baomin; Qu, Jingping
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 19.185 ± 0.002 Å
• b: 11.4028 ± 0.0013 Å
• c: 16.908 ± 0.002 Å
• α: 90°
• β: 99.636 ± 0.002°
• γ: 90°
• Cell volume: 3646.7 ± 0.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0564
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1039
• Weighted residual factors for all reflections included in the refinement: 0.1104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No