Information card for entry 7120746

Structure parameters

• Formula: C39 H81 Ge9 K O Si9
• Calculated formula: C39 H81 Ge9 K O Si9
• Title of publication: TBC - Phil Power's 65th birthday Targeted Attachment of Functional Groups at Ge9 Clusters via Silylation Reactions
• Authors of publication: Mayer, Kerstin; Schiegerl, Lorenz; Kratky, Tim; Guenther, Sebastian; Fässler, Thomas F
• Journal of publication: Chem. Commun.
• Year of publication: 2017
• a: 9.5002 ± 0.0019 Å
• b: 43.372 ± 0.009 Å
• c: 16.273 ± 0.003 Å
• α: 90°
• β: 95.34 ± 0.03°
• γ: 90°
• Cell volume: 6676 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1141
• Residual factor for significantly intense reflections: 0.0662
• Weighted residual factors for significantly intense reflections: 0.1637
• Weighted residual factors for all reflections included in the refinement: 0.1958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No