Crystallography Open Database

Information card for entry 7120968

7120967 << 7120968 >> 7120969

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Coordinates	7120968.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H142 Ge2 Si14
Calculated formula	C74 H142 Ge2 Si14
Title of publication	Reversible addition of terminal alkenes to digermynes.
Authors of publication	Sugahara, Tomohiro; Guo, Jing-Dong; Sasamori, Takahiro; Nagase, Shigeru; Tokitoh, Norihiro
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	5
Pages of publication	519 - 522
a	13.4049 ± 0.0002 Å
b	33.992 ± 0.0009 Å
c	20.3454 ± 0.0004 Å
α	90°
β	91.9033 ± 0.0006°
γ	90°
Cell volume	9265.5 ± 0.3 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1066
Residual factor for significantly intense reflections	0.0809
Weighted residual factors for significantly intense reflections	0.1926
Weighted residual factors for all reflections included in the refinement	0.2073
Goodness-of-fit parameter for all reflections included in the refinement	1.155
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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