Crystallography Open Database

Information card for entry 7120970

7120969 << 7120970 >> 7120971

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Coordinates	7120970.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H146 Ge2 Si14
Calculated formula	C66 H146 Ge2 Si14
Title of publication	Reversible addition of terminal alkenes to digermynes.
Authors of publication	Sugahara, Tomohiro; Guo, Jing-Dong; Sasamori, Takahiro; Nagase, Shigeru; Tokitoh, Norihiro
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	5
Pages of publication	519 - 522
a	14.6873 ± 0.0002 Å
b	17.2952 ± 0.0003 Å
c	18.3289 ± 0.0003 Å
α	92.502 ± 0.001°
β	104.946 ± 0.001°
γ	91.16 ± 0.001°
Cell volume	4491.71 ± 0.13 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0605
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.0924
Weighted residual factors for all reflections included in the refinement	0.1017
Goodness-of-fit parameter for all reflections included in the refinement	1.091
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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