Information card for entry 7121143

Structure parameters

• Common name: (EMind)ClGe=GeCl(EMind)
• Chemical name: dichlorodigermene
• Formula: C48 H74 Cl2 Ge2
• Calculated formula: C48 H74 Cl2 Ge2
• Title of publication: A stable free tetragermacyclobutadiene incorporating fused-ring bulky EMind groups.
• Authors of publication: Suzuki, Katsunori; Numata, Yasuyuki; Fujita, Naoko; Hayakawa, Naoki; Tanikawa, Tomoharu; Hashizume, Daisuke; Tamao, Kohei; Fueno, Hiroyuki; Tanaka, Kazuyoshi; Matsuo, Tsukasa
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 18
• Pages of publication: 2200 - 2203
• a: 10.9924 ± 0.0004 Å
• b: 11.3428 ± 0.0004 Å
• c: 11.8084 ± 0.0005 Å
• α: 118.544 ± 0.004°
• β: 92.15 ± 0.003°
• γ: 113.282 ± 0.003°
• Cell volume: 1140.33 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1116
• Weighted residual factors for all reflections included in the refinement: 0.115
• Goodness-of-fit parameter for all reflections included in the refinement: 1.133
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No