Information card for entry 7121149

Structure parameters

• Formula: C13 H32 Al Li N4 O Si2
• Calculated formula: C13 H32 Al Li N4 O Si2
• Title of publication: Lithium diamidodihydridoaluminates: bimetallic cooperativity in catalytic hydroboration and metallation applications
• Authors of publication: Pollard, Victoria A.; Orr, Samantha A.; McLellan, Ross; Kennedy, Alan R.; Hevia, Eva; Mulvey, Robert E.
• Journal of publication: Chemical Communications
• Year of publication: 2018
• a: 13.3714 ± 0.0007 Å
• b: 14.1997 ± 0.0007 Å
• c: 11.4816 ± 0.0007 Å
• α: 90°
• β: 96.332 ± 0.005°
• γ: 90°
• Cell volume: 2166.7 ± 0.2 ų
• Cell temperature: 160.3 K
• Ambient diffraction temperature: 160.3 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1322
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1915
• Weighted residual factors for all reflections included in the refinement: 0.231
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No