Information card for entry 7121170

Structure parameters

• Formula: C33 H35 N Si
• Calculated formula: C33 H35 N Si
• Title of publication: Palladium-catalyzed primary amine-directed regioselective mono- and di-alkynylation of biaryl-2-amines.
• Authors of publication: Jiang, Guangbin; Hu, Weigao; Li, Jianxiao; Zhu, Chuanle; Wu, Wanqing; Jiang, Huanfeng
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 14
• Pages of publication: 1746 - 1749
• a: 9.0089 ± 0.0006 Å
• b: 13.9567 ± 0.0006 Å
• c: 22.3783 ± 0.001 Å
• α: 98.702 ± 0.004°
• β: 99.193 ± 0.004°
• γ: 99.7 ± 0.004°
• Cell volume: 2691.6 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1029
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1708
• Weighted residual factors for all reflections included in the refinement: 0.1909
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No