Diels-Alder reactions between hexafluoro-2-butyne and bis-furyl dienes: kinetic versus thermodynamic control.
Authors of publication
Borisova, Kseniya K.; Nikitina, Eugeniya V.; Novikov, Roman A.; Khrustalev, Victor N.; Dorovatovskii, Pavel V.; Zubavichus, Yan V.; Kuznetsov, Maxim L.; Zaytsev, Vladimir P.; Varlamov, Alexey V.; Zubkov, Fedor I.
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2018
Journal volume
54
Journal issue
23
Pages of publication
2850 - 2853
a
11.47 ± 0.002 Å
b
18.01 ± 0.004 Å
c
17.04 ± 0.003 Å
α
90°
β
108.15 ± 0.03°
γ
90°
Cell volume
3344.9 ± 1.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0589
Residual factor for significantly intense reflections
0.0451
Weighted residual factors for significantly intense reflections
0.1187
Weighted residual factors for all reflections included in the refinement
0.1288
Goodness-of-fit parameter for all reflections included in the refinement
