Information card for entry 7121255

Structure parameters

• Formula: C27 H49 Cl6.43 O0.58 P2 W
• Calculated formula: C27 H49 Cl7 P2 W
• Title of publication: An unusual alkylidyne homologation.
• Authors of publication: Han, Yong-Shen; Hill, Anthony F.; Kong, Richard Y.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 18
• Pages of publication: 2292 - 2295
• a: 12.31677 ± 0.00014 Å
• b: 14.9414 ± 0.0003 Å
• c: 18.7844 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3456.89 ± 0.1 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0703
• Weighted residual factors for significantly intense reflections: 0.1614
• Weighted residual factors for all reflections included in the refinement: 0.1637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No