Crystallography Open Database

Information card for entry 7121306

Preview

Coordinates	7121306.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H76 As2 Ge
Calculated formula	C55 H76 As2 Ge
Title of publication	A diarsagermylene and a diarsastannylene stabilised by areneGe/Sn interactions.
Authors of publication	Izod, Keith; Evans, Peter; Waddell, Paul G.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	20
Pages of publication	2526 - 2529
a	12.6717 ± 0.0003 Å
b	12.8423 ± 0.0003 Å
c	16.8971 ± 0.0003 Å
α	77.0882 ± 0.0017°
β	78.4162 ± 0.0017°
γ	71.263 ± 0.002°
Cell volume	2513.24 ± 0.1 Å³
Cell temperature	190 ± 0.2 K
Ambient diffraction temperature	190 ± 0.2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0423
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0957
Weighted residual factors for all reflections included in the refinement	0.1008
Goodness-of-fit parameter for all reflections included in the refinement	1.024
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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