Crystallography Open Database

Information card for entry 7121332

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Structure parameters

Formula	C20 H26 N2 O3 S
Calculated formula	C20 H26 N2 O3 S
Title of publication	Construction of α-methoxyimidoyl ketonitrones via phosphite-mediated addition of α-keto N-tert-butanesulfinyl imidates to nitrosoarenes.
Authors of publication	Feng, Jie; Ma, Peng-Ju; Zeng, Yong-Ming; Xu, Yan-Jun; Lu, Chong-Dao
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	23
Pages of publication	2882 - 2885
a	9.546 ± 0.018 Å
b	8.931 ± 0.017 Å
c	12.96 ± 0.02 Å
α	90°
β	107.93 ± 0.02°
γ	90°
Cell volume	1051 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1332
Residual factor for significantly intense reflections	0.0558
Weighted residual factors for significantly intense reflections	0.0925
Weighted residual factors for all reflections included in the refinement	0.1174
Goodness-of-fit parameter for all reflections included in the refinement	1.003
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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