Information card for entry 7121463
| Formula |
C32 H22 Cl2 O3 |
| Calculated formula |
C32 H22 Cl2 O3 |
| Title of publication |
Brønsted Base-Catalyzed Annulation of Allyl Ketones and Alkynyl 1,2-Diketones |
| Authors of publication |
Fang, Xinqiang; Kong, Xiangwen; Liu, Jian; Yang, Shuang; Zeng, Min; Zhan, Xinyue; Li, Chunsen; Song, Jinshuai; Meng, Miao |
| Journal of publication |
Chemical Communications |
| Year of publication |
2018 |
| a |
10.2 ± 0.004 Å |
| b |
21.427 ± 0.007 Å |
| c |
12.408 ± 0.005 Å |
| α |
90° |
| β |
101.29 ± 0.005° |
| γ |
90° |
| Cell volume |
2659.4 ± 1.7 Å3 |
| Cell temperature |
293.15 K |
| Ambient diffraction temperature |
293.15 K |
| Number of distinct elements |
4 |
| Space group number |
4 |
| Hermann-Mauguin space group symbol |
P 1 21 1 |
| Hall space group symbol |
P 2yb |
| Residual factor for all reflections |
0.1667 |
| Residual factor for significantly intense reflections |
0.0698 |
| Weighted residual factors for significantly intense reflections |
0.1272 |
| Weighted residual factors for all reflections included in the refinement |
0.1671 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.993 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7121463.html
