Information card for entry 7121685

Structure parameters

• Formula: C52 H154 B12 Nd2 O P6
• Calculated formula: C52 H154 B12 Nd2 O P6
• Title of publication: Homoleptic uranium and lanthanide phosphinodiboranates.
• Authors of publication: Blake, Anastasia V.; Fetrow, Taylor V.; Theiler, Zachary J.; Vlaisavljevich, Bess; Daly, Scott R.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 44
• Pages of publication: 5602 - 5605
• a: 15.0204 ± 0.0015 Å
• b: 11.9884 ± 0.0012 Å
• c: 24.771 ± 0.002 Å
• α: 90°
• β: 90.05 ± 0.005°
• γ: 90°
• Cell volume: 4460.5 ± 0.7 ų
• Cell temperature: 190 ± 2 K
• Ambient diffraction temperature: 190.15 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0941
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.1604
• Weighted residual factors for all reflections included in the refinement: 0.1817
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No