Information card for entry 7121772

Structure parameters

• Formula: C32 H30 N2 O2
• Calculated formula: C32 H30 N2 O2
• Title of publication: Ytterbium and silver co-catalyzed synthesis of pyrrole-fused bicyclic skeletons from enynones and isocyanides.
• Authors of publication: Li, Feng; Hu, Peng; Sun, Mingming; Li, Chunju; Jia, Xueshun; Li, Jian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 49
• Pages of publication: 6412 - 6415
• a: 7.925 ± 0.005 Å
• b: 12.453 ± 0.007 Å
• c: 13.592 ± 0.008 Å
• α: 83.497 ± 0.008°
• β: 82.328 ± 0.007°
• γ: 88.609 ± 0.008°
• Cell volume: 1320.8 ± 1.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1218
• Residual factor for significantly intense reflections: 0.0833
• Weighted residual factors for significantly intense reflections: 0.2304
• Weighted residual factors for all reflections included in the refinement: 0.2734
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No