Information card for entry 7121814

Structure parameters

• Formula: C26 H37 N O P
• Calculated formula: C26 H37 N O P
• Title of publication: Reductive coupling of two aldehydes to unsymmetrical E-alkenes via phosphaalkene and phosphinate intermediates.
• Authors of publication: Mai, Juri; Arkhypchuk, Anna I.; Gupta, Arvind Kumar; Ott, Sascha
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 52
• Pages of publication: 7163 - 7166
• a: 10.0822 ± 0.0004 Å
• b: 10.8747 ± 0.0004 Å
• c: 12.0033 ± 0.0005 Å
• α: 106.883 ± 0.003°
• β: 90.592 ± 0.003°
• γ: 103.9 ± 0.002°
• Cell volume: 1217.9 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1181
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No