Information card for entry 7121854

Structure parameters

• Formula: C65 H64 B Cl F20 Mg N2 O Si2
• Calculated formula: C65 H64 B Cl F20 Mg N2 O Si2
• Title of publication: Unsupported metal silyl ether coordination.
• Authors of publication: Pahl, Jürgen; Elsen, Holger; Friedrich, Alexander; Harder, Sjoerd
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 56
• Pages of publication: 7846 - 7849
• a: 13.3518 ± 0.0006 Å
• b: 14.4685 ± 0.0007 Å
• c: 17.3377 ± 0.0007 Å
• α: 98.233 ± 0.004°
• β: 97.872 ± 0.004°
• γ: 90.686 ± 0.004°
• Cell volume: 3281.8 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0951
• Weighted residual factors for all reflections included in the refinement: 0.0995
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No