Information card for entry 7121893

Structure parameters

• Formula: C33 H51 N3 Si
• Calculated formula: C33 H51 N3 Si
• Title of publication: An arene-tethered silylene ligand enabling reversible dinitrogen binding to iron and catalytic silylation.
• Authors of publication: Bai, Yunping; Zhang, Jianying; Cui, Chunming
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 58
• Pages of publication: 8124 - 8127
• a: 12.0057 ± 0.0017 Å
• b: 8.9498 ± 0.0011 Å
• c: 15.48 ± 0.002 Å
• α: 90°
• β: 106.694 ± 0.003°
• γ: 90°
• Cell volume: 1593.2 ± 0.4 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0344
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.0925
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No