Information card for entry 7121907

Structure parameters

• Formula: C44 H73 Al N2
• Calculated formula: C44 H73 Al N2
• Title of publication: Reversible 1,1-hydroaluminations and C-H activation in reactions of a cyclic (alkyl)(amino) carbene with alane.
• Authors of publication: Cao, Levy L.; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 60
• Pages of publication: 8407 - 8410
• a: 9.4074 ± 0.0006 Å
• b: 11.461 ± 0.0008 Å
• c: 19.1698 ± 0.0013 Å
• α: 92.871 ± 0.002°
• β: 98.051 ± 0.002°
• γ: 101.38 ± 0.002°
• Cell volume: 1999.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0748
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1159
• Weighted residual factors for all reflections included in the refinement: 0.1295
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No