Crystallography Open Database

Information card for entry 7122186

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Structure parameters

Formula	C19 H20 N2 O
Calculated formula	C19 H20 N2 O
Title of publication	Reductive cyclisations of amidines involving aminal radicals.
Authors of publication	Huang, Huan-Ming; Adams, Ralph W.; Procter, David J.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	72
Pages of publication	10160 - 10163
a	41.133 ± 0.003 Å
b	13.3359 ± 0.0014 Å
c	11.1564 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	6119.8 ± 0.9 Å³
Cell temperature	149.9 ± 0.4 K
Ambient diffraction temperature	149.9 ± 0.4 K
Number of distinct elements	4
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.1087
Residual factor for significantly intense reflections	0.0785
Weighted residual factors for significantly intense reflections	0.1996
Weighted residual factors for all reflections included in the refinement	0.2542
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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