Crystallography Open Database

Information card for entry 7122256

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Structure parameters

Formula	C27 H34 O Si2
Calculated formula	C27 H34 O Si2
Title of publication	Palladium-catalyzed sequential three-component reactions to access vinylsilanes.
Authors of publication	Zhou, Bo; Lu, Ailan; Shao, Changdong; Liang, Xinda; Zhang, Yanghui
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	75
Pages of publication	10598 - 10601
a	9.2327 ± 0.0008 Å
b	9.5206 ± 0.0009 Å
c	17.1628 ± 0.0019 Å
α	94.671 ± 0.004°
β	104.862 ± 0.004°
γ	112.646 ± 0.003°
Cell volume	1318 ± 0.2 Å³
Cell temperature	291 ± 2 K
Ambient diffraction temperature	291 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0669
Residual factor for significantly intense reflections	0.0439
Weighted residual factors for significantly intense reflections	0.1072
Weighted residual factors for all reflections included in the refinement	0.1207
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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