Information card for entry 7122274

Structure parameters

• Formula: C18 H18 Cl2 F6 Ge2 N4 O6 S2
• Calculated formula: C18 H18 Cl2 F6 Ge2 N4 O6 S2
• Title of publication: Bis(chlorogermyliumylidene) and its significant role in elusive reductive cyclization.
• Authors of publication: Majumdar, Moumita; Raut, Ravindra K.; Sahoo, Padmini; Kumar, Vikas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 77
• Pages of publication: 10839 - 10842
• a: 8.3092 ± 0.0011 Å
• b: 13.8633 ± 0.0019 Å
• c: 13.868 ± 0.0019 Å
• α: 64.284 ± 0.004°
• β: 80.304 ± 0.004°
• γ: 73.576 ± 0.004°
• Cell volume: 1378.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.108
• Weighted residual factors for all reflections included in the refinement: 0.1117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No