Information card for entry 7122277

Structure parameters

• Formula: C40 H66 K2 N4 O12
• Calculated formula: C40 H66 K2 N4 O12
• Title of publication: Bis(chlorogermyliumylidene) and its significant role in elusive reductive cyclization.
• Authors of publication: Majumdar, Moumita; Raut, Ravindra K.; Sahoo, Padmini; Kumar, Vikas
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 77
• Pages of publication: 10839 - 10842
• a: 23.5972 ± 0.0019 Å
• b: 14.6704 ± 0.001 Å
• c: 26.824 ± 0.002 Å
• α: 90°
• β: 104.411 ± 0.005°
• γ: 90°
• Cell volume: 8993.8 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.3799
• Residual factor for significantly intense reflections: 0.1133
• Weighted residual factors for significantly intense reflections: 0.1338
• Weighted residual factors for all reflections included in the refinement: 0.1936
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No