Information card for entry 7122336

Structure parameters

• Common name: U(TIG)3
• Formula: C39 H84 N9 U
• Calculated formula: C39 H84 N9 U
• Title of publication: Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane.
• Authors of publication: Settineri, Nicholas S.; Shiau, Angela A.; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 77
• Pages of publication: 10913 - 10916
• a: 13.289 ± 0.0011 Å
• b: 19.9565 ± 0.0016 Å
• c: 18.7099 ± 0.0014 Å
• α: 90°
• β: 110.091 ± 0.003°
• γ: 90°
• Cell volume: 4660 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0589
• Weighted residual factors for all reflections included in the refinement: 0.0622
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No