Information card for entry 7122338

Structure parameters

• Common name: U(Nptolyl)(TIG)3
• Formula: C49 H98 N10 U
• Calculated formula: C49 H98 N10 U
• Title of publication: Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane.
• Authors of publication: Settineri, Nicholas S.; Shiau, Angela A.; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 77
• Pages of publication: 10913 - 10916
• a: 39.246 ± 0.004 Å
• b: 14.3692 ± 0.0016 Å
• c: 19.965 ± 0.002 Å
• α: 90°
• β: 109.062 ± 0.009°
• γ: 90°
• Cell volume: 10642 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0523
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.0987
• Weighted residual factors for all reflections included in the refinement: 0.1043
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No