Information card for entry 7122429

Structure parameters

• Formula: C12 H37.5 Ge9 K0.45 N4.5 O6 Rb3.55
• Calculated formula: C12 H37.5 Ge9 K0.454 N4.5 O6 Rb3.546
• Title of publication: [(μ₂-H)(η²-Ge₄)ZnPh₂]^3-, an edge-on protonated E₄ cluster establishing the first three-center two-electron Ge-H-Ge bond.
• Authors of publication: Henneberger, Thomas; Klein, Wilhelm; Dums, Jasmin V.; Fässler, Thomas F
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 87
• Pages of publication: 12381 - 12384
• a: 38.5713 ± 0.0008 Å
• b: 9.997 ± 0.0002 Å
• c: 19.0042 ± 0.0004 Å
• α: 90°
• β: 94.337 ± 0.002°
• γ: 90°
• Cell volume: 7307 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.044
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.048
• Weighted residual factors for all reflections included in the refinement: 0.05
• Goodness-of-fit parameter for all reflections included in the refinement: 0.924
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No