Crystallography Open Database

Information card for entry 7122453

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Structure parameters

Formula	C42 H32 B3 F10 P
Calculated formula	C42 H32 B3 F10 P
Title of publication	A convenient route to internally phosphane-stabilized aryltriborane(7) compounds.
Authors of publication	Li, Jun; Daniliuc, Constantin G.; Kehr, Gerald; Erker, Gerhard
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	89
Pages of publication	12606 - 12609
a	15.0735 ± 0.0004 Å
b	15.1214 ± 0.0004 Å
c	19.54 ± 0.0006 Å
α	84.907 ± 0.002°
β	81.768 ± 0.002°
γ	86.11 ± 0.001°
Cell volume	4383.6 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1371
Residual factor for significantly intense reflections	0.0832
Weighted residual factors for significantly intense reflections	0.2093
Weighted residual factors for all reflections included in the refinement	0.2374
Goodness-of-fit parameter for all reflections included in the refinement	1.104
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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