Information card for entry 7122540

Structure parameters

• Formula: C112 H160 K2 N4 O10 Yb3
• Calculated formula: C112 H160 K2 N4 O10 Yb3
• Title of publication: Ca(ii), Yb(ii) and Tm(iii) complexes with tri- and tetra-anions of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene.
• Authors of publication: Fedushkin, Igor L.; Lukina, Daria A.; Skatova, Alexandra A.; Lukoyanov, Anton N.; Cherkasov, Anton V.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 92
• Pages of publication: 12950 - 12953
• a: 13.294 ± 0.002 Å
• b: 13.787 ± 0.003 Å
• c: 15.741 ± 0.003 Å
• α: 105.839 ± 0.002°
• β: 92.357 ± 0.002°
• γ: 112.705 ± 0.002°
• Cell volume: 2525.3 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0817
• Residual factor for significantly intense reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.1201
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No