Information card for entry 7122575

Structure parameters

• Formula: C33.09 H43.64 Cl0.73 F2.18 N2.91 O2.18 P1.45 S0.73
• Calculated formula: C33.0909 H43.6364 Cl0.727273 F2.18182 N2.90909 O2.18182 P1.45455 S0.727273
• Title of publication: Taming a silyldiium cation and its reactivity towards sodium phosphaethynolate.
• Authors of publication: Hermannsdorfer, André; Stephan, Douglas W.; Driess, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 96
• Pages of publication: 13523 - 13526
• a: 21.3898 ± 0.0004 Å
• b: 14.7759 ± 0.0002 Å
• c: 32.3467 ± 0.0007 Å
• α: 90°
• β: 108.989 ± 0.002°
• γ: 90°
• Cell volume: 9666.9 ± 0.3 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0725
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.151
• Weighted residual factors for all reflections included in the refinement: 0.1674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No