Information card for entry 7122594

Structure parameters

• Chemical name: IB-365
• Formula: C30 H62 K N3 O3 P2 S4 Si2
• Calculated formula: C30 H62 K N3 O3 P2 S4 Si2
• Title of publication: Expanding the chemistry of ring-fused 1,4-diphosphinines by stable mono anion formation.
• Authors of publication: Begum, Imtiaz; Schnakenburg, Gregor; Kelemen, Zsolt; Nyulászi, László; Boeré, René T; Streubel, Rainer
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 96
• Pages of publication: 13555 - 13558
• a: 8.9737 ± 0.0006 Å
• b: 14.8907 ± 0.0009 Å
• c: 16.9261 ± 0.0011 Å
• α: 77.937 ± 0.005°
• β: 83.96 ± 0.005°
• γ: 88.797 ± 0.005°
• Cell volume: 2199.5 ± 0.2 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1095
• Residual factor for significantly intense reflections: 0.0609
• Weighted residual factors for significantly intense reflections: 0.1395
• Weighted residual factors for all reflections included in the refinement: 0.1544
• Goodness-of-fit parameter for all reflections included in the refinement: 0.859
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No