Information card for entry 7122600

Structure parameters

• Formula: C24 H26 N2 O10 Zn2
• Calculated formula: C24 H26 N2 O10 Zn2
• Title of publication: Diastereoselective solid-state crossed photocycloaddition of olefins in a 3D Zn(ii) coordination polymer.
• Authors of publication: Volodin, Alexander D.; Korlyukov, Alexander A.; Zorina-Tikhonova, Ekaterina N; Chistyakov, Aleksandr S.; Sidorov, Aleksei A.; Eremenko, Igor L.; Vologzhanina, Anna V.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 98
• Pages of publication: 13861 - 13864
• a: 7.1977 ± 0.0004 Å
• b: 24.7844 ± 0.0012 Å
• c: 10.4717 ± 0.0006 Å
• α: 90°
• β: 134.483 ± 0.001°
• γ: 90°
• Cell volume: 1332.78 ± 0.13 ų
• Cell temperature: 300 ± 0.2 K
• Ambient diffraction temperature: 300 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0599
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0797
• Weighted residual factors for all reflections included in the refinement: 0.0879
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No