Information card for entry 7122992

Structure parameters

• Formula: C31 H42 N3 P
• Calculated formula: C31 H42 N3 P
• Title of publication: Unusual ligand rearrangement: from N-phosphinoguanidinato to phosphinimine-amidinato compounds
• Authors of publication: Fernández-Galán, Rafael; Ramos, Alberto; Huergo, Estefanía; Antiñolo, Antonio; Carrillo-Hermosilla, Fernando; Rodríguez-Diéguez, Antonio; García-Vivó, Daniel
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 17.093 ± 0.003 Å
• b: 15.955 ± 0.002 Å
• c: 10.358 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2824.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.0764
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No