Information card for entry 7123334

Structure parameters

• Formula: H62 Mo18 N4 O81 P2
• Calculated formula: Mo18 N4 O83.95 P2
• Title of publication: Synthesis of Polyoxometalate Clusters using Carbohydrates as Reducing Agents Leads to Isomer-Selection
• Authors of publication: Cronin, Lee; Janusson, Eric; Kler, Noel; Vila-Nadal, Laia; Long, Deliang
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.765 ± 0.0008 Å
• b: 15.5376 ± 0.0009 Å
• c: 17.7625 ± 0.001 Å
• α: 82.099 ± 0.003°
• β: 87.537 ± 0.003°
• γ: 83.277 ± 0.003°
• Cell volume: 3735.6 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0465
• Residual factor for significantly intense reflections: 0.0353
• Weighted residual factors for significantly intense reflections: 0.086
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No