Rhodium(II)-catalyzed annulation of N-sulfonyl-1,2,3-triazoles with 1,3,5-triazinanes to produce octahydro-1H-purine derivatives: A combined experimental and computational study
Authors of publication
Ge, Jiemin; Wu, Xueli; Bao, Xiaoguang
Journal of publication
Chemical Communications
Year of publication
2019
a
9.503 ± 0.006 Å
b
10.244 ± 0.007 Å
c
17.165 ± 0.011 Å
α
74.55 ± 0.02°
β
87.703 ± 0.015°
γ
79.93 ± 0.02°
Cell volume
1585.8 ± 1.8 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296.15 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0994
Residual factor for significantly intense reflections
0.0583
Weighted residual factors for significantly intense reflections
0.1447
Weighted residual factors for all reflections included in the refinement
0.1646
Goodness-of-fit parameter for all reflections included in the refinement
