Information card for entry 7123390
| Formula |
C77 H68 B Cl7 F4 N O5 Os P3 |
| Calculated formula |
C77 H68 B Cl7 F4 N O5 Os P3 |
| Title of publication |
Synthesis and Characterization of Metallapentalenoxazetes from the [2+2] Cycloaddition of Metallapentalynes with Nitrosoarenes |
| Authors of publication |
Deng, Zhihong; Zhu, Congqing; Hua, Yuhui; HE, Guomei; Guo, Ying; Lu, Ruqiang; Cao, Xiaoyu; Chen, Jiangxi; Xia, Haiping |
| Journal of publication |
Chemical Communications |
| Year of publication |
2019 |
| a |
12.2871 ± 0.0001 Å |
| b |
14.7115 ± 0.0001 Å |
| c |
21.5051 ± 0.0001 Å |
| α |
93.495 ± 0.001° |
| β |
103.864 ± 0.001° |
| γ |
101.686 ± 0.001° |
| Cell volume |
3671.23 ± 0.05 Å3 |
| Cell temperature |
100 ± 0.1 K |
| Ambient diffraction temperature |
100 ± 0.1 K |
| Number of distinct elements |
9 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0447 |
| Residual factor for significantly intense reflections |
0.0384 |
| Weighted residual factors for significantly intense reflections |
0.1015 |
| Weighted residual factors for all reflections included in the refinement |
0.1048 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.051 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
1.54184 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/7123390.html
