Information card for entry 7123867

Structure parameters

• Formula: C39 H50 As N3 Si
• Calculated formula: C39 H50 As N3 Si
• Title of publication: Reaction of an arsinoamide with chloro tetrylenes: substitution and As‒N bond insertion
• Authors of publication: Chen, Xiao; Simler, Thomas; Yadav, Ravi; Gamer, Michael T.; Köppe, Ralf; Roesky, Peter W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 16.8814 ± 0.0004 Å
• b: 12.7921 ± 0.0003 Å
• c: 18.4683 ± 0.0005 Å
• α: 90°
• β: 116.297 ± 0.002°
• γ: 90°
• Cell volume: 3575.46 ± 0.17 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0612
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1126
• Weighted residual factors for all reflections included in the refinement: 0.1222
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No