Information card for entry 7123904

Structure parameters

• Formula: C15 H24 F O5 P Si2 W
• Calculated formula: C15 H24 F O5 P Si2 W
• Title of publication: Competitive or sequential reaction of an electrophilic terminal phosphinidene metal(0) complex with allyl halides? [2+1]-Cycloaddition vs C-X bond insertion
• Authors of publication: Khan, Arif; Junker, Philip; Schnakenburg, Gregor; Espinosa, Arturo; Streubel , R.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 9.4372 ± 0.0003 Å
• b: 18.8621 ± 0.0006 Å
• c: 12.3957 ± 0.0004 Å
• α: 90°
• β: 94.0074 ± 0.0018°
• γ: 90°
• Cell volume: 2201.11 ± 0.12 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0619
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1483
• Weighted residual factors for all reflections included in the refinement: 0.1529
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No